|
05/03/2015, 05:33 PM | #1 |
BlueWorldAquatics.com
Join Date: May 2012
Location: Murrieta, CA
Posts: 657
|
Milwaukee Digital Refractometer
I am having a problem getting my Milwaukee Digital Refractometer to calibrate once I ran out of the 1.000 SG solution provided with the kit.
I have tried using RODI water and water I steam distilled myself. All show a SG of 1.030 when I calibrate with the 1.026 solution I have. Steps I do every time: 1. Put distilled water in the meter, enough to cover up the eye. 2. Hit zero on the meter, shows 1.000 on the meter 3. Wipe out the distilled water with cloth I got from my manual refractometer 4. Put 1.026 solution in the meter, enough to cover the eye. 5. Hit Read. It shows 1.030 Is there another step I am missing? Shouldn't it know 1.026 once it is zeroed? I have just been making my tank water so that I reads the same reading as the 1.026 calibration solution. Things in the tank look good, just spent a lot of money on the digital refractometer, because I was tired of trying to figure out which line on the manual refractometer to use as the reading. Hope I can get this working again.
__________________
Stats: 180 g Mixed SPS/LPS reef tank, 30 gallon sump, live rock, GFO\Carbon, AquaMaxx AM250 in-sump skimmer, felt filter socks, cleaning crew |
05/03/2015, 06:17 PM | #2 |
Registered Member
Join Date: Aug 2014
Location: Angola, Indiana
Posts: 235
|
I'm guessing your not using solution provided by Milwaukee to check it against since your not using their calibration fluid? If not that's most likely your problem.
If you don't have any you'll need to email them and they'll send it out free of charge. |
05/03/2015, 06:32 PM | #3 |
Registered Member
Join Date: Dec 2006
Location: Brantford ON. Canada
Posts: 277
|
Well that OK I zero mine and tried the solution that they supplied with the unit and I get 1.023 and the solution should be 1.025,then I test my tank and the Milwaukee says 1.024 and my Red Sea unit says 1.026. Now tell me which one would you believe.
Skim |
05/04/2015, 10:07 AM | #4 |
BlueWorldAquatics.com
Join Date: May 2012
Location: Murrieta, CA
Posts: 657
|
[QUOTE=water is wet;23717823]I'm guessing your not using solution provided by Milwaukee to check it against since your not using their calibration fluid? If not that's most likely your problem.
If you don't have any you'll need to email them and they'll send it out free of charge.[/QUOTE Can I get this from their website? I dont think MarineDepot or BRS has it
__________________
Stats: 180 g Mixed SPS/LPS reef tank, 30 gallon sump, live rock, GFO\Carbon, AquaMaxx AM250 in-sump skimmer, felt filter socks, cleaning crew |
05/04/2015, 11:19 AM | #5 |
Saltwater Addict
Join Date: Jan 2012
Location: Vandalia OHIO
Posts: 11,624
|
I calibrate mine with RO water and have never used the calibration solution they supply. The meter has a correction factor of +-.002
__________________
Fish are not disposable commodities, but a worthwhile investment that can be maintained and enjoyed for many years, providing one is willing to take the time to understand their requirements and needs Current Tank Info: 625g, 220g sump, RD3 230w, Vectra L1 on a closed loop, 3 MP60s, MP40. Several QTs |
05/04/2015, 11:56 AM | #6 | |
BlueWorldAquatics.com
Join Date: May 2012
Location: Murrieta, CA
Posts: 657
|
Quote:
__________________
Stats: 180 g Mixed SPS/LPS reef tank, 30 gallon sump, live rock, GFO\Carbon, AquaMaxx AM250 in-sump skimmer, felt filter socks, cleaning crew |
|
05/04/2015, 12:11 PM | #7 | |
Saltwater Addict
Join Date: Jan 2012
Location: Vandalia OHIO
Posts: 11,624
|
Quote:
__________________
Fish are not disposable commodities, but a worthwhile investment that can be maintained and enjoyed for many years, providing one is willing to take the time to understand their requirements and needs Current Tank Info: 625g, 220g sump, RD3 230w, Vectra L1 on a closed loop, 3 MP60s, MP40. Several QTs |
|
05/04/2015, 12:21 PM | #8 | |
BlueWorldAquatics.com
Join Date: May 2012
Location: Murrieta, CA
Posts: 657
|
Quote:
__________________
Stats: 180 g Mixed SPS/LPS reef tank, 30 gallon sump, live rock, GFO\Carbon, AquaMaxx AM250 in-sump skimmer, felt filter socks, cleaning crew |
|
05/04/2015, 01:02 PM | #9 |
Saltwater Addict
Join Date: Jan 2012
Location: Vandalia OHIO
Posts: 11,624
|
If the solution is off then your salinity in the tank will also be off by whatever it is (in this case.004 it sounds like) what I don't understand is if you use RO water and it reads 1.000 why when you read the calibration solution it's so far off?
__________________
Fish are not disposable commodities, but a worthwhile investment that can be maintained and enjoyed for many years, providing one is willing to take the time to understand their requirements and needs Current Tank Info: 625g, 220g sump, RD3 230w, Vectra L1 on a closed loop, 3 MP60s, MP40. Several QTs |
05/04/2015, 01:09 PM | #10 | |
BlueWorldAquatics.com
Join Date: May 2012
Location: Murrieta, CA
Posts: 657
|
Quote:
__________________
Stats: 180 g Mixed SPS/LPS reef tank, 30 gallon sump, live rock, GFO\Carbon, AquaMaxx AM250 in-sump skimmer, felt filter socks, cleaning crew |
|
05/04/2015, 01:56 PM | #11 |
Saltwater Addict
Join Date: Jan 2012
Location: Vandalia OHIO
Posts: 11,624
|
No the light in the room shouldn't matter at all
__________________
Fish are not disposable commodities, but a worthwhile investment that can be maintained and enjoyed for many years, providing one is willing to take the time to understand their requirements and needs Current Tank Info: 625g, 220g sump, RD3 230w, Vectra L1 on a closed loop, 3 MP60s, MP40. Several QTs |
05/04/2015, 02:12 PM | #12 | |
Registered Member
Join Date: Aug 2014
Location: Angola, Indiana
Posts: 235
|
Quote:
After receiving their solution they both work perfect again. |
|
05/04/2015, 02:33 PM | #13 | |
BlueWorldAquatics.com
Join Date: May 2012
Location: Murrieta, CA
Posts: 657
|
Quote:
__________________
Stats: 180 g Mixed SPS/LPS reef tank, 30 gallon sump, live rock, GFO\Carbon, AquaMaxx AM250 in-sump skimmer, felt filter socks, cleaning crew |
|
05/04/2015, 02:40 PM | #14 |
Registered Member
Join Date: Aug 2014
Location: Angola, Indiana
Posts: 235
|
There is no charge. As far as I know they are the only ones to carry it.
http://www.milwaukeeinstruments.com/...ct-information Sales and Support In The United States Only* Milwaukee Instruments, Inc. 2950 Business Park Drive Rocky Mount, NC 27804 - U.S.A. Tel.: 1.252.443.3630 Fax: 1.252.443.1937 Primary:*sales@milwaukeeinstruments.com Financial Dept:*accounting@milwaukeeinstruments.com Technical Dept:*support@milwaukeeinstruments.com* |
05/04/2015, 03:35 PM | #15 |
Saltwater Addict
Join Date: Jan 2012
Location: Vandalia OHIO
Posts: 11,624
|
Thanks for the info. Do you have to call someone to get the solution, I'm not seeing it?
__________________
Fish are not disposable commodities, but a worthwhile investment that can be maintained and enjoyed for many years, providing one is willing to take the time to understand their requirements and needs Current Tank Info: 625g, 220g sump, RD3 230w, Vectra L1 on a closed loop, 3 MP60s, MP40. Several QTs |
05/04/2015, 04:13 PM | #16 |
Registered Member
Join Date: Nov 2014
Posts: 134
|
I have one of these same refractometers, and it reads .001 high very consistently. For purposes of a water change, you technically don't even need to calibrate it, as long as the new water reads whatever your old water reads.
As far as knowing the actual SG, the thing you need to make absolutely sure of with a "test liquid" is that it has the same refractive properties of 1.026 seawater. Some liquids are made for calibrating a salinity probe at 53mS. While this is the same resistance as 1.026 seawater, the fluid will not have the same refractive index as 1.026 seawater. I calibrate to 1.000 with the solution provided (until its gone), barely ever calibrate it to be honest. It doesn't seem to drift much. I then check it with a fluid with a known refractive index of 1.026. It always reads 1.027. I know that if my aquarium tests at 1.027, it is actually around 1.026. Ambient light can affect the readings. I try to use it away from any strange colored artificial light. If I don't believe the reading, I will shield the sensor from ambient light, and it has changed in the past. Also, you have to realize that it takes a little time, 30 secs to a minute for the temp of the water to be the same as the temp of the sensor, this is important because temp affects the reading as well. It usually goes up if you wait a minute. Also make sure there are no bubbles in the water on the sensor. I also cover the sensor a lot, so the water is covering a portion of the edge of the metal dish surrounding the crystal. |
05/04/2015, 04:29 PM | #17 |
BlueWorldAquatics.com
Join Date: May 2012
Location: Murrieta, CA
Posts: 657
|
I emailed Milwaukee Instruments. I will let everyone know what they say about getting more calibration fluid
__________________
Stats: 180 g Mixed SPS/LPS reef tank, 30 gallon sump, live rock, GFO\Carbon, AquaMaxx AM250 in-sump skimmer, felt filter socks, cleaning crew |
05/04/2015, 04:37 PM | #18 |
Registered Member
Join Date: Jan 2014
Location: Alsip, IL
Posts: 1,133
|
I ran into trouble calibrating mine. The unit I received had a card, along with the instructions, stating to use only distilled water and not ro/di water. Even though the instructions read ro/di. I first used distilled water from Walgreens and was finding inconsistent results. I then tried ro/di water with a TDS reading of 0 and again, was not getting good results. After making my own distilled water, I can get consistent results using a commercial seawater sample. It is a pain sometimes, but this is what I have to do get get the same result over and over.
__________________
Four legs good. Two legs better. Current Tank Info: 50G SPS/NPS Reef, 120G Mixed Reef, 120G FOWRL, 29G Seahorse tank, 20G Observation tank, |
05/04/2015, 04:41 PM | #19 |
BlueWorldAquatics.com
Join Date: May 2012
Location: Murrieta, CA
Posts: 657
|
I did make my own steam distiller water on the stove expecting to see my 1.026 calibration solution show 1.026 but it showed 1.030. The calibration solution I am using is from American Marine Pinpoint. It is 53.0 mS standardized fluid
__________________
Stats: 180 g Mixed SPS/LPS reef tank, 30 gallon sump, live rock, GFO\Carbon, AquaMaxx AM250 in-sump skimmer, felt filter socks, cleaning crew |
05/04/2015, 04:58 PM | #20 |
Registered Member
Join Date: Nov 2014
Posts: 134
|
That's interesting. I also use American Marine 53mS solution, as it is supposed to also be 1.026 refractive index. I always get 1.027 as mentioned above.
Have you ever left that bottle open? Evaporation could affect the actual SG of the solution. |
05/04/2015, 05:45 PM | #21 |
Registered Member
Join Date: Aug 2014
Location: Angola, Indiana
Posts: 235
|
|
05/04/2015, 05:48 PM | #22 |
Team RC member
|
With a standard error of the mean of +/- 0.002 you should get reproducibility constrained by the accuracy of the instrument. I would, for example, not use this as a measure of the accuracy of hyposalinity.
__________________
Warmest regards, ~Steve~ |
05/04/2015, 07:29 PM | #23 | |
Saltwater Addict
Join Date: Jan 2012
Location: Vandalia OHIO
Posts: 11,624
|
Quote:
__________________
Fish are not disposable commodities, but a worthwhile investment that can be maintained and enjoyed for many years, providing one is willing to take the time to understand their requirements and needs Current Tank Info: 625g, 220g sump, RD3 230w, Vectra L1 on a closed loop, 3 MP60s, MP40. Several QTs |
|
05/06/2015, 07:14 AM | #24 |
Registered Member
Join Date: Aug 2014
Location: Angola, Indiana
Posts: 235
|
Have either of you heard back?
|
05/06/2015, 09:14 AM | #25 | |
Registered Member
Join Date: Apr 2015
Location: South East England - UK
Posts: 213
|
Quote:
All I do is add the mixed water to the reader, hit read and bosh 1.026 provided I measured my salt correctly.
__________________
Success is not final, failure is not fatal. It is the courage to continue that counts - Sir Winston Churchill Current Tank Info: Juwel Trigon 190, Clearseal Astra sump, Maxspect Grye 150, AI Hydra, Bubble Magus 5.5 Skimmer and GFO reactor and Eheim 3000 return. |
|
Tags |
distilled water, milwaukee digital, refractometer calibration, rodi |
|
|